EBSD技术已成为表征大多数金属、合金、复合材料和陶瓷微观组织的主要工具，这也可能是EBSD应用的最大领域。其应用范围非常广泛，从轧制金属板中晶粒尺寸和织构的常规（以及现在的快速）测量，到与裂纹扩展相关的位错密度的详细分析。这些材料中，有许多比较容易使用EBSD分析，但诸如TKD或高分辨率花样的相关性分析等高级工具，正越来越多地应用，以提高我们对这些材料的理解。这些应用的关键在于，这些材料的物理性能与微观组织参数之间的密切关系。这些微观组织参数可以通过EBSD技术轻松表征。以下的列表给出了此领域中的一些典型应用，尽管完整的应用范围要大得多：
超级双相不锈钢的相分布图，在矿物油中处理以模拟海水环境，以研究金属间化合物相对应力腐蚀开裂的影响。图中黄色是σ相，蓝色是γ相而红色是α相。箭头标识了某些裂纹，显示了裂纹在σ相中产生，并沿着γ相晶粒扩展，被α相和γ相阻断。
Discover how EBSD can be used to characterise the dislocation type and densities in deformed metals and alloys, enabling a better understanding of the material’s physical properties. Here we compare 2 deformed Ti alloys, showing how advanced dislocation analysis using AZtecCrystal highlights the operation of different slip systems during deformation.
Learn how parent grain microstructures can be reconstructed from low temperature EBSD analyses using AZtecCrystal. Here, the reconstruction results for a Titanium sample are tested using in-situ EBSD analyses of beta-Ti collected at >900 °C using a new type of high temperature phosphor screen. The results indicate an excellent agreement between the as-measured and reconstructed beta-Ti microstructures.
The extreme analysis speed achievable with the Symmetry S2 EBSD detector enables effective characterisation of samples at speeds over 4500 indexed patterns per second. Here a deformed and heat-treated Ni sheet is analysed using EBSD in just a few minutes, providing all key microstructural measurements.
The grain size is an important parameter of a material, it will strongly affect mechanical and physical properties. Understanding how grain size is influenced through the processing of materials, can assist in engineering materials with optimised properties.
Microanalysis is a powerful tool in understanding potential failure mechanisms and potential life time of many materials. In this example, the microstructure and damage distribution following creep deformation of a nickel superalloy is studied using EBSD and EDS
This application note illustrates the application of TKD to a nanostructured nickel sample and a highly deformed stainless steel, both of which were impossible to characterise using conventional EBSD.
Careful sample preparation enables good quality EBSD data to be collected from an alumina insulator. This data provides valuable information on the microstructure of the material – in particular grain size and distribution, texture and porosity.
The Symmetry detector is ideal for the routine characterisation of metal samples at speeds up to 3000 pps. Here it is used to characterise a deformed Ni superalloy and a large area across a welded duplex steel.
This technical note illustrates the capability of Oxford Instruments AZtecSynergy microanalysis system using the Tru-I® indexing engine to perform Phase Identification.
Here the high analysis speed of the Symmetry S2 EBSD detector is combined with the advanced data processing capability of AZtecCrystal to characterise the complex phase distribution in 2 quenching and partitioning (Q&P) processed high strength steels.
In this webinar, where are joined by one of the developers of a new approach to parent grain reconstruction, Dr Hung-Wei (Homer) Yen, who will be discussing the importance of understanding parent microstructures in the steel industry.
Learn how the combination of EDS & EBSD on an electron microscope can be applied to the characterisation of materials ensuring manufacturing and product reliablity.
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